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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1434530Generated: October 28, 2026

Tributylphosphine → HCID 86605960, compound

https://huagongshe.com/reaction/1434530

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTributylphosphineHCID 13831—
ReactantDi-tert-butyl azodicarboxylateHCID 97268—
ReactantHCID 86605961HCID 86605961—
SolventTetrahydrofuranHCID 8028—
ProductHCID 86605960HCID 86605960—

Reaction Steps

Prepared analogously to Example 2c from benzyl (R)-[1-hydroxymethyl-2-(6-methyl-5-nitro-pyridin-2-yl-carbamoyl)-ethyl]-carbamate with di-tert.-butyl azodicarboxylate and tributylphosphine in THF and subsequent purification by reversed-phase chromatography.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07615549B2
Source datasetuspto-grants-2009_11
ORD IDord-c1f113cc69714ce7ba7bed2e1e32066b
Source noteuspto-grants-2009_11