Triacetoxyperiodinane → HCID 57935958, compound

Participants

Reaction Steps

To a solution of (3R)-3-(3,5-difluorophenyl)-3-(1,1-dioxidotetrahydro-2H-thiopyran-4-yl)propan-1-ol (1.26 g) in dichloromethane (10 ml) was added Dess-Martin periodinane (588 mg) in one portion. The resulting mixture was stirred at room temperature for 2 hours. The mixture was partitioned between 1N NaOH solution and dichloromethane. The organics were dried and evaporated to give the title compound as an oil, which was subsequently used without further purification.

Provenance & Evidence