p-Fluoronitrobenzene → HCID 21904799, compound

HRID 1434722Notes

Reaction equation

HRID 1434722 reaction equation
[CH:1]12[N:8]([C:9]3[CH:15]=[CH:14][C:12]([NH2:13])=[CH:11][CH:10]=3)[CH:5]([CH2:6][CH2:7]1)[CH2:4][CH2:3][CH2:2]2.[F:16]C1C=CC([N+]([O-])=O)=CC=1>>[CH:5]12[N:8]([C:9]3[CH:10]=[CH:11][C:12]([NH2:13])=[CH:14][C:15]=3[F:16])[CH:1]([CH2:7][CH2:6]1)[CH2:2][CH2:3][CH2:4]2

Participants

3

Reactant 2

HCID 9590p-FluoronitrobenzeneHCID 21904779HCID 21904779, compound

Product 1

HCID 21904799HCID 21904799, compound

Procedure

The title compound was prepared using the procedure as described for the preparation of the product of Example 6B, substituting 3,4-difluoronitrobenzene for 4-fluoronitrobenzene 1H NMR (300 MHz, CDCl3) δ 6.69 (m, 1H), 6.40 (m, 2H), 4.00 (brs, 2H), 3.42 (brs, 2H), 1.86-2.03 (m, 4H), 1.65-1.77 (m, 3H), 1.32-1.57 (m, 3H).

Sources & evidence

ORD record
ord-3fb234dab93348d88ea82e4f7ac8fc5e
Source dataset
uspto-grants-2009_11
Patent number
US07615570B2

Reaction notes

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