HCID 23709820, compound → HCID 57936516, compound

HRID 1434872Notes

Reaction equation

HRID 1434872 reaction equation
F[C:2]1[CH:11]=[CH:10][C:5]([C:6]([O:8][CH3:9])=[O:7])=[C:4]([O:12]COC)[CH:3]=1.[CH2:16]([S-:19])[CH2:17][CH3:18].[K+]>>[OH:12][C:4]1[CH:3]=[C:2]([S:19][CH2:16][CH2:17][CH3:18])[CH:11]=[CH:10][C:5]=1[C:6]([O:8][CH3:9])=[O:7]

Participants

3

Reactant 2

HCID 23709820HCID 23709820, compoundHCID 58437341Methyl 4-fluoro-2-(methoxymethoxy)benzoate

Product 1

HCID 57936516HCID 57936516, compoundYield 55%

Procedure

Using a procedure analogous to Example 66-A, methyl 4-fluoro-2-(methoxymethoxy)benzoate and potassium propanethiolate gave the title compound (6.1 g, 55%).

Sources & evidence

ORD record
ord-4effaa53b8644f4bbb4b35de3f6862d1
Source dataset
uspto-grants-2009_11
Patent number
US07615568B2

Reaction notes

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