3-(Tributylstannyl)pyridine → [4-(5-Pyridin-3-yl-thiophen-2-yl)-pyrimidin-2-yl]-(2,2,6,6-tetramethyl-piperidin-4-yl)-amine

Participants

Role	Name	HCID	Charge
Reactant	3-(Tributylstannyl)pyridine	HCID 3483848	—
Reactant	{4-[5-Bromothiophen-2-yl]-pyrimidin-2-yl}-(2,2,6,6-tetramethyl-piperidin-4-yl)-amine	HCID 57936128	—
Product	[4-(5-Pyridin-3-yl-thiophen-2-yl)-pyrimidin-2-yl]-(2,2,6,6-tetramethyl-piperidin-4-yl)-amine	HCID 11292323	38%

Reaction Steps

The title compound was prepared as described for Example 25, using [4-(5-bromo-thiophen-2-yl)-pyrimidin-2-yl]-(2,2,6,6-tetramethyl-piperidin-4-yl)-amine (Step C of Example 5) and 3-tributylstannylpyridine. Yield: 38%.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07615562B2
Source dataset	uspto-grants-2009_11
ORD ID	ord-cd17dc838a20494e992e4dffe0c7e35a
Source note	uspto-grants-2009_11