huagongshe.com
HRID1435035

反应详情

EQUATION

反应方程式

HRID 1435035 的结构方程式

REACTANTS

反应物

3
结构：CCCC[N+](CCCC)(CCCC)CCCC.[F-]
HCID2724141

Tetra-n-butylammonium fluoride

C16H36FN

结构：CC(C)(C)[Si](C)(C)n1ccc2cccnc21
HCID10847211

1-(tert-butyl-dimethyl-silanyl)-1H-pyrrolo[2,3-b]pyridine

C13H20N2Si

结构：CC1(C)CC(Nc2nccc(Cl)n2)CC(C)(C)N1
HCID57936167

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)CC(Nc2nccc(-c3c[nH]c4ncccc34)n2)CC(C)(C)N1
HCID57936321

未命名化合物

PROCEDURE

实验过程

The title compound was prepared as described in Example 215, starting from 1-(tert-butyl-dimethyl-silanyl)-1H-pyrrolo[2,3-b]pyridine (prepared by TBDMS protection of 1H-pyrrolo[2,3-b]pyridine) and (4-chloro-pyrimidin-2-yl)-(2,2,6,6-tetramethyl-piperidin-4-yl)-amine, followed by in situ cleavage of the TBDMS protecting group with catalytic amounts of TBAF.