HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 11548237, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 5(S)-[1(S)-Azido-3(S)-[4-methoxy-3-(3-methoxypropoxy)benzyl]-4-methylpentyl]-3(S)-isopropyldihydrofuran-2-one | HCID 11775573 | — |
| Product | HCID 11548237 | HCID 11548237 | — |
Reaction Steps
Analogously to Method C, 0.466 g of 5(S)-{1(S)-azido-3(S)-[4-methoxy-3-(3-methoxypropoxy)benzyl]-4-methylpentyl}-3(S)-isopropyidihydrofuran-2-one [324763-46-4] and 0.11 ml of aniline are reacted. The title compound is obtained as a colourless oil. Rf=0.53 (2:1 EtOAc-heptane); Rt=5.41 minutes (gradient I).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615664B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-56c614e48c0347c19cea42ffe3fb197d |
| Source note | uspto-grants-2009_11 |