HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → Heneicosane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 2-Heneicosanone | HCID 529805 | — |
| Solvent | Ethylene Glycol | HCID 174 | — |
| Product | Heneicosane | HCID 12403 | — |
Reaction Steps
reacting 2,4-alkaneanedione with 1-bromooctadecane in absolute ethanol in the presence of 18-crown-6 as catalyst to produce 2-heneicosanone; and (b) reducing said 2-heneicosanone using hydrazine hydrate and potassium hydroxide in ethylene glycol to obtain n-heneicosane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615672B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-08319e4891cc4395bcc05204abe4d5cb |
| Source note | uspto-grants-2009_11 |