HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54695617, compound → HCID 68569908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54695617 | HCID 54695617 | — |
| Reactant | HCID 57937626 | HCID 57937626 | — |
| Product | HCID 68569908 | HCID 68569908 | 73.3% |
Reaction Steps
Title compound (2.2 g) was prepared from methyl 5-(1H-benzimidazol-1-yl)-3-hydroxy-2-thiophenecarboxylate (J. Heterocyclic Chem., 1987, 24, 1301-1303) (1.9 g, 7.0 mmol) and (1S)-1-(2-chloro-3-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}phenyl)ethanol (Intermediate 17, 2.0 g, 7.0 mmol) using a procedure analogous to Intermediate 2, Step C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615643B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-9633f67c773848d3a7a89182699fd28b |
| Source note | uspto-grants-2009_11 |