HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57937558, compound → HCID 57937479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57937558 | HCID 57937558 | — |
| Reactant | HCID 59855195 | HCID 59855195 | — |
| Product | HCID 57937479 | HCID 57937479 | 98.1% |
Reaction Steps
The title compound was prepared from methyl 5-(5-bromo-1H-benzimidazol-1-yl)-3-hydroxy-2-thiophenecarboxylate (0.64 g, 1.8 mmol) and 1,1-dimethylethyl 4-({2-chloro-3-[(1S)-1-hydroxyethyl]phenyl}oxy)-1-piperidinecarboxylate (0.78 g, 2.2 mmol) using a procedure analogous to Intermediate 2, Step C to give 1.22 g of the desired product. MS (ESI): 692.4 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615643B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-bfc21596b9ed44df9cbc20d74a89916c |
| Source note | uspto-grants-2009_11 |