HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-[cis-4-(Boc-amino)cyclohexyl]methanesulfonamide → HCID 86760349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-[cis-4-(Boc-amino)cyclohexyl]methanesulfonamide | HCID 18348373 | — |
| Reactant | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 86760349 | HCID 86760349 | — |
Reaction Steps
The compound obtained from step A was dissolved in 50% trifluoroacetic acid/dichloromethane and the mixture was stirred at room temperature for 30 minutes. The excess acid was removed under reduced pressure and the residue was triturated with ether to give a white powder, 1.51 g, 90% for two steps. MS(ES) (M+H)+=193.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615634B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-f57b0cf0c101441f8022fa5ce043a83a |
| Source note | uspto-grants-2009_11 |