HRID1435551

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID178447926

未命名化合物

反应SMILES：CC[C@H]1CC[C@H](CC(=O)OC(C)(C)C)CC1

HCID178455749

未命名化合物

PRODUCTS

产物

反应SMILES：CCC[C@H]1CC[C@H](C(O)CCC(C(=O)OC(C)(C)C)[C@H]2CC[C@H](CC)CC2)CC1

HCID178448089

未命名化合物

收率 85.3%

PROCEDURE

实验过程

Reaction operations were carried out according to the first step of Example 1 by using 1-(trans-4-propylcyclohexyl)oxetane (37) (3.1 g, 17.0 mmol) and tert-butyl 2-(trans-4-ethylcyclohexyl)acetate (40) (12.3 g, 54.4 mmol) as starting materials to obtain tert-butyl 2-(trans-4-ethylcyclohexyl)-5-hydroxy-5-(trans-4-propylcyclohexyl)pentanoate (41) (6.8 g, 14.5 mmol). The yield based on the compound (37) was 85%.

WORKUP

后处理

customReaction operations