HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 178526787, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | 5-Nitropyridine-2,3-diamine | HCID 3480151 | — |
| Solvent | Nitrobenzene | HCID 7416 | — |
| Product | HCID 178526787 | HCID 178526787 | — |
Reaction Steps
14.05 g 2,3-diamino-5-nitropyridine and 9.68 g benzaldehyde in 250 ml nitrobenzene were heated to 140-150° C. for 15 hrs. The solvent is removed by vacuum distillation and the residue is dispersed in ethyl acetate, filtered, and the filter residue washed thoroughly with ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618964B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-2a21a9b8f79d4fa5808affebe05e0531 |
| Source note | uspto-grants-2009_11 |