HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-(Diethylamino)-Ethoxy)-Benzaldehyde → HCID 178464071, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-(Diethylamino)-Ethoxy)-Benzaldehyde | HCID 411674 | — |
| Reactant | 5-Bromopyridine-2,3-diamine | HCID 691156 | — |
| Solvent | Nitrobenzene | HCID 7416 | — |
| Product | HCID 178464071 | HCID 178464071 | — |
Reaction Steps
3.31 g 5-bromo-2,3-diaminopyridine and 3.90 g 4-(2-diethylaminoethoxy)-benzaldehyde in 120 ml nitrobenzene were heated to 140-150° C. for 24 hrs. The solvent was removed by vacuum distillation. The residue was dispersed in ethyl acetate and the crude product was isolated by filtration and washed thoroughly with more ethyl acetate. Yield 1.45 g
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618964B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-0c1a36683a934de29462bac35ea2edb0 |
| Source note | uspto-grants-2009_11 |