3-Chlorobenzenesulphonyl chloride → HCID 9925082, compound

HRID 1435616Notes

Reaction equation

HRID 1435616 reaction equation
[NH2:1][C:2]1[S:3][CH:4]=[C:5]([CH2:7][C:8]([O:10][CH2:11][CH3:12])=[O:9])[N:6]=1.[Cl:13][C:14]1[CH:15]=[C:16]([S:20](Cl)(=[O:22])=[O:21])[CH:17]=[CH:18][CH:19]=1>>[Cl:13][C:14]1[CH:15]=[C:16]([S:20]([NH:1][C:2]2[S:3][CH:4]=[C:5]([CH2:7][C:8]([O:10][CH2:11][CH3:12])=[O:9])[N:6]=2)(=[O:22])=[O:21])[CH:17]=[CH:18][CH:19]=1

Participants

3

Reactant 2

HCID 179093-Chlorobenzenesulphonyl chlorideHCID 1044544-Thiazoleacetic acid, 2-amino-, ethyl ester

Product 1

HCID 9925082HCID 9925082, compound

Procedure

The title compound was prepared from ethyl 2-amino-4-thiazolylacetate and 3-chlorobenzenesulfonyl chloride according to METHOD A, giving 0.47 g (65%) of a pink powder: MS (electrospray, [M−H]−) m/z 359.1.

Sources & evidence

ORD record
ord-546bf8fbf82b4ac3a6cc746faad1f0f3
Source dataset
uspto-grants-2009_11
Patent number
US07618961B2

Reaction notes

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