Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Chloro-2-methylbenzenesulfonyl chloride → Methyl (2-{[(3-chloro-2-methylphenyl)sulfonyl]amino}-5-methyl-1,3-thiazol-4-yl)acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Chloro-2-methylbenzenesulfonyl chloride | HCID 522734 | — |
| 반응물 | Methyl 2-(2-amino-5-methyl-1,3-thiazol-4-yl)acetate | HCID 2763571 | — |
| 생성물 | Methyl (2-{[(3-chloro-2-methylphenyl)sulfonyl]amino}-5-methyl-1,3-thiazol-4-yl)acetate | HCID 86594953 | — |
반응 단계
The title compound was prepared from methyl 2-(2-amino-5-methyl-1,3-thiazol-4-yl)acetate and 3-chloro-2-methylbenzenesulfonyl chloride as described in the synthetic METHOD B to give a white solid (23.2 mg) with purity >90%. LCMS (pos) m/z 375.2.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07618961B2 |
| 출처 데이터셋 | uspto-grants-2009_11 |
| ORD ID | ord-259cae2180724468aaea4a556ffa5cae |
| 출처 메모 | uspto-grants-2009_11 |