HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dichlorobenzoic acid → 2,4-Dichloro-6-(2,5-dichlorophenyl)-1,3,5-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dichlorobenzoic acid | HCID 5784 | — |
| Reactant | 2,4-Dichloro-6-(5-chloro-2-methyl-phenyl)-[1,3,5]triazine | HCID 85827032 | — |
| Product | 2,4-Dichloro-6-(2,5-dichlorophenyl)-1,3,5-triazine | HCID 20480386 | 14% |
Reaction Steps
Using the method described for the synthesis of 2,4-dichloro-6-(5-chloro-2-methyl-phenyl)-[1,3,5]triazine, 2,5-dichlorobenzoic acid afforded 2,4-dichloro-6-(2,5-dichloro-phenyl)-[1,3,5]triazine (2.2 g, 14% yield). 1H NMR (DMSO-d6) 8.10 (s, 1H), 7.50 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618968B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-0e171e5dcf604b95ac974cec699bd988 |
| Source note | uspto-grants-2009_11 |