HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Morpholinoethylamine → HCID 11223120, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Morpholinoethylamine | HCID 408285 | — |
| Reactant | 2-chloro-N-(4-methoxyphenyl)-N-methylquinazolin-4-amine | HCID 11738112 | — |
| Product | HCID 11223120 | HCID 11223120 | — |
Reaction Steps
The title compound was prepared from (2-chloro-quinazolin-4-yl)-(4-methoxy-phenyl)-methyl-amine (10 mg, 0.033 mmol) and 2-morpholin-4-yl-ethylamine (30 μL) by a procedure similar to example 10 and was isolated as white powder (10 mg, 100%). 1H NMR (CDCl3): 7.42 (dd, J=8.7 and 1.2 Hz, 1H), 7.36 (ddd, J=8.1, 6.6 and 1.5 Hz, 1H), 7.10-7.09 (m, 2H), 6.92-6.86 (m, 3H), 6.67 (ddd, J=8.1, 6.6 and 1.4 Hz, 1H), 3.82 (s, 3H), 3.75-3.62 (m, 6H), 3.52 (s, 3H), 2.55-2.44 (m, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07618975B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-492e97260e5f480588f26ac231a35f13 |
| Source note | uspto-grants-2009_11 |