HRID14368

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8148

N-Butyl-1-butanamine

C8H19N

结构：CCCN(CCC)c1ccc2nc3ccccc3[s+]c2c1.CCCN(CCC)c1ccc2nc3ccccc3[s+]c2c1.CCCN(CCC)c1ccc2nc3ccccc3[s+]c2c1.[I-].[I-].[I-]

HCID178457153

未命名化合物

PRODUCTS

生成物

结构：CCCCN(CCCC)c1ccc2nc3ccc(N(CCC)CCC)cc3[s+]c2c1.[I-]

HCID178449028

未命名化合物

PROCEDURE

实验过程

This compound was obtained following isolation of 3-(N,N-dipropylamino)-phenothiazin-5-ium triiodide and subsequent treatment with dibutylamine. Precipitation from dichloromethane by addition of diethyl ether yielded purple lustrous crystals. Mass spectrometry: C26H35N3OS requires m/z=424; found m/z=424 (I− not detected by mass spectrometry).

WORKUP

后处理

customThis compound was obtained
customPrecipitation from dichloromethane
additionby addition of diethyl ether yielded purple lustrous crystals

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-926d37582d884ac098708bb8d28739ba
来源数据集: uspto-grants-2010_06
DOI: 10.6084/m9.figshare.5104873.v1
专利: US07732439B2
来源说明: uspto-grants-2010_06

反应 SMILES

[I-:1].[I-].[I-].[CH2:4]([N:7]([C:11]1[CH:12]=[CH:13][C:14]2[C:23]([CH:24]=1)=[S+:22][C:21]1[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=1)[N:15]=2)[CH2:8][CH2:9][CH3:10])[CH2:5][CH3:6].C(N([C:32]1[CH:33]=[CH:34][C:35]2C(C=1)=[S+]C1[C:37](=[CH:38][CH:39]=[CH:40]C=1)[N:36]=2)CCC)CC.C(N(C1C=CC2C(C=1)=[S+]C1C(=CC=CC=1)N=2)CCC)CC.C(NCCCC)CCC>>[I-:1].[CH2:35]([N:36]([C:19]1[CH:18]=[CH:17][C:16]2[C:21]([CH:20]=1)=[S+:22][C:23]1[C:14](=[CH:13][CH:12]=[C:11]([N:7]([CH2:8][CH2:9][CH3:10])[CH2:4][CH2:5][CH3:6])[CH:24]=1)[N:15]=2)[CH2:37][CH2:38][CH2:39][CH3:40])[CH2:34][CH2:33][CH3:32]