HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 57939223, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 57939225 | HCID 57939225 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57939223 | HCID 57939223 | 99.5% |
Reaction Steps
500 μL of 1 N sodium hydroxide solution (500 μmol) are added portionwise to 80 mg of 29 (263 μmol) in methanol (3 mL). The solution is refluxed for 24 hours. After evaporating off the solvent, the reaction medium is acidified with 0.5 N HCl and extracted with DCM. 76 mg of a yellow oil are obtained, i.e. a yield of 99%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07619076B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-adab0d2197484393a68796a07ea8463d |
| Source note | uspto-grants-2009_11 |