HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23069873, compound → HCID 22047906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23069873 | HCID 23069873 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22047906 | HCID 22047906 | 104.7% |
Reaction Steps
The resulting benzyl 4-(cyclopropylmethyl)homopiperazin-1-carboxylate (2.5 g) was dissolved in 50 mL of ethanol, 10% palladium-carbon (500 mg) was added, and the reaction mixture was stirred at room temperature under hydrogen atmosphere (1 atm) for 12 hours. The palladium-carbon was removed by filtration, and the filtrate was evaporated to give the title compound (1.4 g) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07619100B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-a96de5e5835c4e7caff3336e1e92bbec |
| Source note | uspto-grants-2009_11 |