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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1436982Generated: October 31, 2026

HCID 23069873, compound → HCID 22047906, compound

https://huagongshe.com/reaction/1436982

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 23069873HCID 23069873—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 22047906HCID 22047906104.7%

Reaction Steps

The resulting benzyl 4-(cyclopropylmethyl)homopiperazin-1-carboxylate (2.5 g) was dissolved in 50 mL of ethanol, 10% palladium-carbon (500 mg) was added, and the reaction mixture was stirred at room temperature under hydrogen atmosphere (1 atm) for 12 hours. The palladium-carbon was removed by filtration, and the filtrate was evaporated to give the title compound (1.4 g) as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07619100B2
Source datasetuspto-grants-2009_11
ORD IDord-a96de5e5835c4e7caff3336e1e92bbec
Source noteuspto-grants-2009_11