HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,6-Dimethylpiperazine → 8-Chloro-11-(3,5-dimethyl-piperazin-1-yl)-5H-dibenzo[b,e][1,4]diazepine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,6-Dimethylpiperazine | HCID 66056 | — |
| Edukt | 8-chloro-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 3653116 | — |
| Produkt | 8-Chloro-11-(3,5-dimethyl-piperazin-1-yl)-5H-dibenzo[b,e][1,4]diazepine | HCID 135477948 | 52,8% |
Reaktionsschritte
8-Chloro-5,10-dihydro-dibenzo[b,e][1,4]diazepine-11-one (25 mg, 0.1 mmol) and 2,6-dimethylpiperazine (114 mg, 1.0 mmol) were reacted according to GP4 to give 18 mg of the title compound (160FE33B). MS (ESI) 341 (MH+). Purity for MH+ (UV/MS) 100/100.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07622461B2 |
| Quelldatensatz | uspto-grants-2009_11 |
| ORD ID | ord-ab783fb84c184016b49aa41d91998f61 |
| Quellennotiz | uspto-grants-2009_11 |