HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68630790, compound → HCID 135620682, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68630790 | HCID 68630790 | — |
| Reactant | HCID 136056013 | HCID 136056013 | — |
| Product | HCID 135620682 | HCID 135620682 | 42% |
Reaction Steps
8-Chloro-11-methylsulfanyl-5H-dibenzo[b,e][1,4]diazepine (166JO50) (50 mg, 0.11 mmol) and N-(tert-butoxycarbonylamino)-2,5-diazabicyclo[2.2.1]heptane (34 mg, 0.2 mmol) were reacted according to GP8 to give 15 mg of the title compound (166JO39-2). MS (ESI) 324 (MH+). Purity for MH+ (UV/MS) 93/100.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622461B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-4adbcdead655438b9fe582d59bd9aebf |
| Source note | uspto-grants-2009_11 |