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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1437037Generated: October 30, 2026

B-(4-Nonylphenyl)boronic acid → 8-Chloro-11-(4-nonylphenyl)-5H-dibenzo[b,e][1,4]diazepine

https://huagongshe.com/reaction/1437037

Reaction equation

Participants

RoleNameHCIDCharge
ReactantB-(4-Nonylphenyl)boronic acidHCID 4589192—
Reactant8,5-Dichloro-5H-dibenzo[b,e][1,4]diazepineHCID 57485431—
Product8-Chloro-11-(4-nonylphenyl)-5H-dibenzo[b,e][1,4]diazepineHCID 13605601458%

Reaction Steps

4-Nonylphenylboronic acid (30 mg, 0.12 mmol) and 8,5-dichloro-5H-dibenzo[b,e][1,4]diazepine (160FE64) (26 mg, 0.1 mmol) were reacted according GP11 to give 25 mg of the title compound (160FE63). MS (ESI) 431 (MH+). Purity for MH+ (UV/MS) 85/85.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07622461B2
Source datasetuspto-grants-2009_11
ORD IDord-5ec465b440424d4dab919cbffd7f2088
Source noteuspto-grants-2009_11