HRID1437216

反应详情

EQUATION

反应方程式

HRID 1437216 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

10% Palladium-carbon (50% wet, 90 mg) was added to 5-nitro-2-vinylpyridine (450 mg) in ethanol (30 mL), followed by stirring in a hydrogen atmosphere at room temperature for 15 hours. The catalyst was removed from the reaction mixture by filtration. Subsequently, the solvent was evaporated under reduced pressure, to thereby give the title compound as an oily substance (359 mg, 98%).

WORKUP

后处理

  1. customThe catalyst was removed from the reaction mixture by filtration
  2. customSubsequently, the solvent was evaporated under reduced pressure