HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-chloropyridine N-oxide → 4-Chloro-2-pyridinecarbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-chloropyridine N-oxide | HCID 70724 | — |
| Reactant | Trimethylsilyl cyanide | HCID 82115 | — |
| Product | 4-Chloro-2-pyridinecarbonitrile | HCID 693342 | 92% |
Reaction Steps
The general procedure of Referential Example 15 was repeated through use of 4-chloropyridine-N-oxide (6.00 g) and trimethylsilyl cyanide (17.5 mL), to thereby give the title compound as a solid (5.89 g, 92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622471B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-2e40be9fa26e4f989ded74a0260e4fac |
| Source note | uspto-grants-2009_11 |