HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Oxalate → Ethyl 4-(4-fluorophenyl)-2,4-dioxobutanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Oxalate | HCID 7268 | — |
| Reactant | 4'-Fluoroacetophenone | HCID 9828 | — |
| Product | Ethyl 4-(4-fluorophenyl)-2,4-dioxobutanoate | HCID 596593 | 60% |
Reaction Steps
The general procedure of Referential Example 3-1) was repeated through use of 4′-fluoroacetophenone (3.0 g) and diethyl oxalate (5.9 mL), to thereby give the title compound as a solid (3.12 g, 60%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622471B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-fb0310f8678d4f4ba3c5dc3f164fb826 |
| Source note | uspto-grants-2009_11 |