HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 68699270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 57941060 | HCID 57941060 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68699270 | HCID 68699270 | 122.6% |
Reaction Steps
A solution of ester (c) (1.5 g) in methanol (50 mL) was treated with lithium hydroxide (630 mg). After 2 hours acetic acid (1 mL) was added and the mixture was evaporated to dryness. Chromatography on silica eluting with 1:9:90 (acetic acid:methanol:dichloromethane) afforded an oil (1.02 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622481B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-9c27ce1ba6ab4d75af38d3f90bf92473 |
| Source note | uspto-grants-2009_11 |