HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 22499224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 8-Hydroxy-6-methylquinolin-2(1H)-one | HCID 22499171 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 22499224 | HCID 22499224 | — |
Reaction Steps
A 45% solution of hydrobromic acid in acetic acid (324 μL) is added dropwise to a solution of 8-hydroxy-6-methyl-1H-quinolin-2-one (316 mg) in dimethylsulphoxide (9 mL) at room temperature. The reaction mixture is allowed to stand for 18 hours at room temperature and the solvent removed in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622483B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-984b0eb0f5684b4487c10aaa6003d0ac |
| Source note | uspto-grants-2009_11 |