HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2,6-Dichlorophenyl)hydrazine monohydrochloride → (2,6-Dichlorophenyl)hydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2,6-Dichlorophenyl)hydrazine monohydrochloride | HCID 2723909 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Sodium chloride; water | HCID 57417360 | — |
| Product | (2,6-Dichlorophenyl)hydrazine | HCID 84634 | 101.8% |
Reaction Steps
A mixture of 2,6-dichloro-phenylhydrazine hydrochloride (11.7 g, 54.8 mmol) in 1 M NaOH (55 mL), brine (200 mL) and saturated sodium bicarbonate (100 mL) was extracted with dichloromethane (3×200 mL). The organic layers were combined, dried (sodium sulfate), filtered and evaporated to give 2,6-dichloro-phenylhydrazine (9.88 g, quantitative).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07622492B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-04f35371dfd24e64af3908f466f24987 |
| Source note | uspto-grants-2009_11 |