HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1438095Generated: October 26, 2026
Iodine chloride → 5-Iodo-2-isopropoxyphenyl acetate
https://huagongshe.com/reaction/1438095
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Iodine chloride | HCID 24640 | — |
| Reactant | 2-Isopropoxyphenyl acetate | HCID 57073664 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 5-Iodo-2-isopropoxyphenyl acetate | HCID 58789145 | — |
Reaction Steps
To a solution of 2-isopropoxyphenyl acetate (10 mmol) in CH2Cl2 at 0° C., iodine monochloride (1.0 M in CH2Cl2, 11.0 mL) was added dropwise in 20 min. The mixture was stirred at 0° C. for 2.0 h, diluted with ether, washed with saturated Na2S2O3 and brine. The organic extract was dried over MgSO4 and evaporated to give 5-iodo-2-isopropoxyphenyl acetate as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07622585B2 |
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| Source dataset | uspto-grants-2009_11 |
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| ORD ID | ord-bcd87e29c2af43c5bd06116d2c147a5a |
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| Source note | uspto-grants-2009_11 |
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