HCID 22752998, compound → HCID 54471858, compound

HRID 1438707Notes

Reaction equation

HRID 1438707 reaction equation
I.[CH3:2][NH:3][C:4](=[NH:7])[S:5][CH3:6].[CH:8]([N:11]([C:15](Cl)=[O:16])[C:12](Cl)=[O:13])([CH3:10])[CH3:9]>>[CH:8]([N:11]1[C:15](=[O:16])[NH:7][CH:4]([S:5][CH3:6])[N:3]([CH3:2])[C:12]1=[O:13])([CH3:10])[CH3:9]

Participants

3

Reactant 2

HCID 22752998HCID 22752998, compoundHCID 178485204HCID 178485204, compound

Product 1

HCID 54471858HCID 54471858, compound

Procedure

Analogously to Example 24, N,S-dimethyl-isothiourea hydroiodide and N-isopropyl-bis-(chlorocarbonyl)-amine (prepared analogously to Synthesis 1970, pages 542-543; boiling point 66-67° C/12 mm Hg yielded 1-isopropyl-3-methyl-4-methylmercapto-tetrahydro-1,3,5-triazine-2,6-dione as a colorless powder of melting point 73°-75° C.

Sources & evidence

ORD record
ord-aab146ca42d341e18c47ad3d7dafa76e
Source dataset
uspto-grants-1977_11
Patent number
US04056527

Reaction notes

Loading…