HCID 21400252, compound → HCID 54555341, compound

HRID 1438708Notes

Reaction equation

HRID 1438708 reaction equation
I.[CH3:2][NH:3][C:4](=[NH:7])[S:5][CH3:6].[CH:8]1([N:14]([C:18](Cl)=[O:19])[C:15](Cl)=[O:16])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1>>[CH:8]1([N:14]2[C:18](=[O:19])[NH:7][CH:4]([S:5][CH3:6])[N:3]([CH3:2])[C:15]2=[O:16])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1

Participants

3

Reactant 2

HCID 21400252HCID 21400252, compoundHCID 178485204HCID 178485204, compound

Product 1

HCID 54555341HCID 54555341, compound

Procedure

Analogously to Example 24, N,S-dimethyl-isothiourea hydroiodide and N-cyclohexyl-bis-(chlorocarbonyl)-amine (prepared analogously to Synthesis 1970, pages 542-543; boiling point 80°-82° C/0.3 mm Hg) yielded 1-cyclohexyl-3-methyl-4-methylmercapto-tetrahydro-1,3,5-triazine-2,6-dione as a colorless powder of melting point 135°-137° C.

Sources & evidence

ORD record
ord-1980cc3c2cd94aef9227d8d035c2adba
Source dataset
uspto-grants-1977_11
Patent number
US04056527

Reaction notes

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