Maleic Acid → HCID 22766925, compound

HRID 1438739Notes

Reaction equation

HRID 1438739 reaction equation
[CH3:1][C:2]1([CH2:15][CH2:16][N:17]2[CH2:22][CH2:21]N(C)[CH2:19][CH2:18]2)[C:7]2[NH:8][C:9]3[C:14]([C:6]=2[CH2:5][CH2:4][O:3]1)=[CH:13][CH:12]=[CH:11][CH:10]=3.C(O)(=O)/C=C\C(O)=O>>[CH3:1][C:2]1([CH2:15][CH2:16][N:17]2[CH2:18][CH2:19][CH2:21][CH2:22]2)[C:7]2[NH:8][C:9]3[C:14]([C:6]=2[CH2:5][CH2:4][O:3]1)=[CH:13][CH:12]=[CH:11][CH:10]=3

Participants

3

Reactant 2

HCID 444266Maleic AcidHCID 22766952HCID 22766952, compound

Product 1

HCID 22766925HCID 22766925, compound

Procedure

1-methyl-1-[2-(4-methyl-1-piperazinyl)ethyl]-1,3,4,9-tetrahydropyrano[3,4-b]indole, nmr (CDC13) δ1.47 (3H), 2.58 (3H), 3.87 (t,2H), [m.p. of corresponding maleic acid addition salt (i.e. dimaleate), 208° - 210° C.], respectively.

Sources & evidence

ORD record
ord-6168f26c464844778aaa4762230070a0
Source dataset
uspto-grants-1977_11
Patent number
US04056537

Reaction notes

Loading…