HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 70601995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 86733773 | HCID 86733773 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | HCID 70601995 | HCID 70601995 | 67% |
Reaction Steps
An 0.80 g (3.01 mmol) portion of the 5-ethoxycarbonyl-7-methyl-3-methylthio-2-oxindole in 130 ml of absolute ethanol was treated with Raney Nickel by the above described procedure to give 0.44 g (2.01 mmol, 67% yield) of 5-ethoxycarbonyl-7-methyl-2-oxindole, m.p. 238°-241°;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04056569 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-59778359ce584edcb10172d494c38c29 |
| Source note | uspto-grants-1977_11 |