HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Acetoxy-3-dimethylamino-1,1-diphenyl-propane → 3-Dimethylamino-1,1-diphenyl-propan-2-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Acetoxy-3-dimethylamino-1,1-diphenyl-propane | HCID 12549121 | — |
| Solvent | Potassium Hydroxide | HCID 14797 | — |
| Product | 3-Dimethylamino-1,1-diphenyl-propan-2-ol | HCID 12549122 | 99% |
Reaction Steps
2-Acetoxy-3-dimethylamino-1,1-diphenyl-propane (200mg) was dissolved in methanolic potassium hydroxide (5% 10 ml) and the solution allowed to stand overnight. Solvent was evaporated and the residue dissolved in ether and water. The ether extract was dried and evaporated to give 3-dimethylamino-1,1-diphenyl-propan-2-ol (170 mg, 97%), m.p. 72° - 73°
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04056630 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-f48f0051f0b4455daeff666c3b196fcf |
| Source note | uspto-grants-1977_11 |