Dimethylamine → HCID 21399293, compound

HRID 1438841Notes

Reaction equation

HRID 1438841 reaction equation
[NH2:1][N:2]1[C:7](=[O:8])[C:6]([CH:9]([CH2:11][CH3:12])[CH3:10])=[N:5][N:4]=[C:3]1SC.[CH3:15][NH:16][CH3:17]>>[NH2:1][N:2]1[C:7](=[O:8])[C:6]([CH:9]([CH2:11][CH3:12])[CH3:10])=[N:5][N:4]=[C:3]1[N:16]([CH3:17])[CH3:15]

Participants

3

Reactant 2

HCID 674DimethylamineHCID 23050531HCID 23050531, compound

Product 1

HCID 21399293HCID 21399293, compoundYield 93%

Procedure

Analogously to the procedure described in Example 5, reaction of 42.8 g of 4-amino-6-sec.-butyl-3-methylthio-1,2,4-triazin-5 (4H)-one with dimethylamine gave 39.4 g (93% of theory) of 4-amino-6-sec.-butyl-3-dimethylamino-1,2,4-triazin-5 (4H)-one in the form of a viscous oil.

Sources & evidence

ORD record
ord-5095bfd28c724da283289765ea909713
Source dataset
uspto-grants-1977_11
Patent number
US04057417

Reaction notes

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