HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrogen Peroxide → 1-Methyl-3-(4-cyano-3-(methylsulfinyl)-5-isothiazolyl)urea
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrogen Peroxide | HCID 784 | — |
| Edukt | 1-Methyl-3-(4-cyano-3-(methylthio)-5-isothiazolyl)urea | HCID 21399276 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Produkt | 1-Methyl-3-(4-cyano-3-(methylsulfinyl)-5-isothiazolyl)urea | HCID 21399266 | — |
Reaktionsschritte
The reaction was repeated using 24.2 of 1-methyl-3-(4-cyano-3-(methylthio)-5-isothiazolyl)urea and 12 ml of 30% hydrogen peroxide in 175 ml of acetic acid to give 7.9 g of 1-methyl-3-(4-cyano-3-(methylsulfinyl)-5-isothiazolyl)urea, m.p. 241° (decomposes).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04057416 |
| Quelldatensatz | uspto-grants-1977_11 |
| ORD ID | ord-68177961688a421e9917661ef9a69380 |
| Quellennotiz | uspto-grants-1977_11 |