反应详情

温度

50 °C

To a mixture of 0.046 g of zirconium tetrachloride and 0.113 g of 2-dimethylaminobenzyllithium was added 3 ml of toluene, and the mixture was warmed to about 50° C with stirring. Reaction slowly took place to give an orange liquid. When there was no further appreciable change in the color of the liquid, the mixture was cooled and filtered to give an orange solution of tetrakis(2-dimethylaminobenzyl)zirconium.

1. customReaction slowly took place
2. customto give an orange liquid
3. temperaturethe mixture was cooled
4. filtrationfiltered