Benzoyl Peroxide → HCID 86735185, compound

HRID 1438946Notes

Reaction equation

HRID 1438946 reaction equation
[CH:1]([N:3]1[CH:7]=[CH:6][N:5]=[CH:4]1)=[CH2:2].[C:8]([O:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])(=[O:11])[CH:9]=[CH2:10].C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>C1(C)C=CC=CC=1>[CH:1]([N:3]1[CH:7]=[CH:6][N:5]=[CH:4]1)=[CH2:2].[C:8]([O:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])(=[O:11])[CH:9]=[CH2:10]

Participants

5

Reactant 3

HCID 7187Benzoyl PeroxideHCID 661711-VinylimidazoleHCID 75084Lauryl acrylate

Product 1

HCID 86735185HCID 86735185, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Conditions

Temperature
60 °C

Procedure

23.5 gm (0.25 mol) of N-vinylimidazole and 179.75 gm (0.75 mol) of lauryl acrylate were dissolved in 480 gm of toluene. 4 gm of dibenzoylperoxide were added as a catalyst to the solution obtained. The reaction mixture was agitated for 6 hours at 60° C. After the reaction had been completed, the solvent was distilled off and the product was washed a few times with methanol. 162 gm, that is 80% of theory, of N-vinylimidazole/lauryl acrylate copolymer (1:3) were obtained.

Workup

  1. customobtained
  2. distillationthe solvent was distilled off
  3. washthe product was washed a few times with methanol

Sources & evidence

ORD record
ord-e38fb1360f96474cb32cc7bc0a5a6fd8
Source dataset
uspto-grants-1977_11
Patent number
US04057622

Reaction notes

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