HCID 12428590, compound → HCID 178449189, compound

HRID 1438967Notes

Reaction equation

HRID 1438967 reaction equation
[CH2:1]([N:5]=[C:6]=[N:7][C:8]1[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=1)[CH2:2][CH2:3][CH3:4].C([N:18]=[C:19]=[N:20]C1C=NC=CC=1)(C)(C)C>>[CH2:1]([NH:5][C:6]([NH:7][C:8]1[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=1)=[N:20][C:19]#[N:18])[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 12428590HCID 12428590, compoundHCID 54452698HCID 54452698, compound

Product 1

HCID 178449189HCID 178449189, compound

Procedure

By following the procedure of Example 1, but substituting N-n-Butyl-N'-3-pyridylcarbodiimide for the N-tert-butyl-N'-3-pyridylcarbodiimide, the desired compound was obtained with a melting point of 96.0°-97.0° C.

Sources & evidence

ORD record
ord-b56077387d16409dbb8db3061ba2e6a9
Source dataset
uspto-grants-1977_11
Patent number
US04057636

Reaction notes

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