HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20330460, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Mepiroxol | HCID 71668 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20330460 | HCID 20330460 | — |
Reaction Steps
A solution of 30 g. of 3-hydroxymethylpyridine-N-oxide in 200 ml. of benzene and 18.4 g. of thionyl chloride was refluxed 2 hours, cooled and filtered to give 3-mercaptomethylpyridine-N-oxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04057637 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-c52881bd469247adb09a107fd297f787 |
| Source note | uspto-grants-1977_11 |