Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Butanedioic acid, 2-mercapto-, 1,4-dibutyl ester | HCID 97984 | — |
| Catalyst | Titanium tetrabutoxide | HCID 21801 | — |
| Product | HCID 86735193 | HCID 86735193 | — |
Reaction Steps
Two moles dibutyl thiomalate, 1 mole ethylene glycol, and 3 g tetrabutyl titanate catalyst were stirred and heated for 3 hours at 125° C. Vacuum was then applied, and volatiles stripped off to 135° C and 18 mm, to give butyl ethylene thiomalate having the following properties:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04058543 |
|---|
| Source dataset | uspto-grants-1977_11 |
|---|
| ORD ID | ord-59925ec54abb4b25991ff5455ee27782 |
|---|
| Source note | uspto-grants-1977_11 |
|---|
