Maleic Anhydride → Sodium methyl maleate
Reaction equation
[C:1]1(=[O:7])[O:6][C:4](=[O:5])[CH:3]=[CH:2]1.[C:8](=O)([O-])[O-:9].[Na+:12].[Na+]>CO>[C:4]([O:9][CH3:8])(=[O:5])/[CH:3]=[CH:2]\[C:1]([O-:6])=[O:7].[Na+:12]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
1 mole of maleic anhydride is dissolved in 1000 ml methanol and 0.5 mole of sodium carbonate is added. The solution is filtered and the methanol is distilled off under pressure. After drying the product in a vacuum oven 152 g of sodium methyl maleate is obtained.
Workup
- filtrationThe solution is filtered
- distillationthe methanol is distilled off under pressure
- dry with materialAfter drying the product in a vacuum oven 152 g of sodium methyl maleate
- customis obtained
Sources & evidence
- ORD record
- ord-5dd4f4004b984e498a04901a399e0061
- Source dataset
- uspto-grants-1977_11
- Patent number
- US04058554
Reaction notes
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