HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetonitrile → HCID 20393696, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetonitrile | HCID 7856 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | (2,3-Dichloro-4-hydroxyphenyl)(phenyl)methanone | HCID 14009997 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20393696 | HCID 20393696 | — |
Reaction Steps
A mixture of 26.70 g. (0.10 mole) of 4-benzoyl-2,3-dichlorophenol, 7.40 g. (0.10 mole) of chloroaceto nitrile, 10.40 g. (0.15 mole) of anhydrous K2CO3 and catalytic amount of KI in 200 ml. of acetone was refluxed overnight. The residue was triturated with ether and the product was collected by filtration and dried to yield 22.80 g. (75%); m.p. 110°-112°. This product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04058559 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-a6cb90a5f50c4dedba1a89701683a8a0 |
| Source note | uspto-grants-1977_11 |