化工社化工社 化学情報印刷レポート · 研究参考用
Thymol → (-)-Menthol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thymol | HCID 6989 | — |
| 反応物 | (+)-Menthol | HCID 165675 | — |
| 反応物 | (+)-Neomenthol | HCID 439263 | — |
| 生成物 | (-)-Menthol | HCID 16666 | — |
反応手順
Mixtures of 50 to 70 % by weight of thymol with 50 to 30 % by weight of d-neomenthol or d-menthol were used as starting material in accordance with the general conditions described above. In Table I below, column 1 gives the composition of the starting material, column 2 the balance yield of d,l-menthol in percent of the theoretical, whilst the other columns give the contents in the reaction product of d,l-neomenthol, d,l-isomenthol, menthone and other ketones, also hydrocarbons, the OH-number, the optical rotation and the thymol content, calculated from the UV-absorption.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04058571 |
| 出典データセット | uspto-grants-1977_11 |
| ORD ID | ord-7aa69fc0c11744fc810509713aa1d418 |
| 出典メモ | uspto-grants-1977_11 |