HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-1,2-propanediol → 2,3-Dihydroxypropyl 4-(n-hexadecylamino)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-1,2-propanediol | HCID 7290 | — |
| Reactant | Cetaben Sodium | HCID 23703815 | — |
| Solvent | Hexamethylphosphoramide | HCID 12679 | — |
| Product | 2,3-Dihydroxypropyl 4-(n-hexadecylamino)benzoate | HCID 13019380 | — |
Reaction Steps
A solution of 57.5 g of sodium 4-(n-hexadecylamino)benzoate and 55.0 g of 3-chloro-1,2-propanediol in 350 ml of hexamethylphosphoramide is treated in the manner described in Example 3 to yield 2,3-dihydroxypropyl 4-(n-hexadecylamino)benzoate melting at 112°-113° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04058550 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-2ff07c8b4ee64a528d0ecfd9172fc7c1 |
| Source note | uspto-grants-1977_11 |