HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-1,2-propanediol → HCID 21326950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-1,2-propanediol | HCID 7290 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 20556316 | HCID 20556316 | — |
| Solvent | Hexamethylphosphoramide | HCID 12679 | — |
| Product | HCID 21326950 | HCID 21326950 | — |
Reaction Steps
A solution of 6.36 g. of 4-(n-tridecylamino)benzoic acid in 25 ml. of hexamethylphosphoramide is treated with sodium hydride and the 1-chloro-2,3-propanediol in the manner described in Example 2 to yield 2,3-dihydroxypropyl 4-(n-tridecylamino)benzoate as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04058550 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-587096fa384d41e3acba3a405ce846d4 |
| Source note | uspto-grants-1977_11 |