反应详情

A solution of 7.66 g. of sodium 4-(n-hexadecylamino)benzoate and 12.1 g. of allyl bromide in 100 ml. of dry hexamethylphosphoramide is added to a reaction flask. After 6 hours the solution is poured into 100 ml. of water and the solid collected and recrystallized from 50 ml. of acetonitrile. This material is recrystallized from hexanol to yield the title compound, m.p. 81°-83° C.

1. additionAfter 6 hours the solution is poured into 100 ml
2. customof water and the solid collected
3. customrecrystallized from 50 ml
4. customThis material is recrystallized from hexanol