HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanesulfonylchloride, 2-chloro- → HCID 21396800, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanesulfonylchloride, 2-chloro- | HCID 15385 | — |
| Reactant | Dimethyl (2-hydroxyethyl)phosphonate | HCID 2733833 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 21396800 | HCID 21396800 | — |
Reaction Steps
Dimethyl 2-vinylsulfonyloxyethylphosphonate was prepared in the same way as in Example 1 from 3.8 g of dimethyl 2-hydroxyethylphosphonate, 1.9 g of pyridine and 4.0 g of 2-chloroethylsulfonyl chloride. The yield was 20 mol%. The NMR spectrum (CDCl3) of this product was as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04059432 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-62596728e2b541f7b9403d1969fbee66 |
| Source note | uspto-grants-1977_11 |